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Title:
Process for preparing methyl ester of O,O-dimethyl-dithiophosphoryl acetic acid
Abstract:
The methyl ester of O,O-dimethyl-dithiophosphoryl acetic acid is prepared with minimal formation of by-products by reacting the sodium salt of O,O-dimethyl-dithiophosphoryl acid with the methyl ester of 2-chloroacetic acid at a pH of 5.5 to 7, at relatively high temperatures, of the order of 80.degree. to 100.degree. C, for reaction times of 10 to 15 minutes. The process can be carried out continuously.
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Inventors:
Bornengo, Mario (Mestre, IT) Grego, Saverio (Mestre, IT)
Application Number:
560201
Filing Date: 1975-03-20 Publication_date: 1976-12-14 Assignee:
Montedison Fibre S.p.A. (Milan, IT)
Primary Class(es):
558/107
987/209
Other Classes:
US Patent Ref:
| 2358133 | Sep, 1944 | Stoesser et al. | 260/990. | | 3047459 | Jul, 1962 | Perini et al. | 260/979. | | 3591666 | Jul, 1971 | Pellegrini et al. | 260/990. |
Other Refs:
Primary Examiner:
Sutto, Anton H.
Assistant Examiner:
Attorney:
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