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Title: Purification of dinitrotoluene

Abstract: 2,4- AND 2,6-Dinitrotoluenes are separated from mixtures thereof with small mounts of isomeric dinitrotoluene impurities by suspending the mixture in an aqueous solution containing a small amount of an alkali metal disulfide. The isomeric dinitrotoluene impurities are thereby converted to products soluble in the aqueous solution from which the 2,4- and 2,6-dinitrotoluenes can be recovered in excellent yield.


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Inventors: Rosenblatt, David H. (Baltimore, MD, US)
Dennis, Jr., William H. (Braddock Heights, MD, US)

Application Number: 529873
Filing Date: 1974-12-05
Publication_date: 1976-01-06
Assignee: The United States of America as represented by the Secretary of the Army (Washington, DC)
Primary Class(es): 568/934
Other Classes:
US Patent Ref:
Other Refs: 459,169
Feb, 1970JA

Primary Examiner: Sebastian, Leland A.
Assistant Examiner:
Attorney: Edelberg; Nathan, Gibson; Robert P., Erkkila; A. Victor