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Title:
Purification of dinitrotoluene
Abstract:
2,4- AND 2,6-Dinitrotoluenes are separated from mixtures thereof with small mounts of isomeric dinitrotoluene impurities by suspending the mixture in an aqueous solution containing a small amount of an alkali metal disulfide. The isomeric dinitrotoluene impurities are thereby converted to products soluble in the aqueous solution from which the 2,4- and 2,6-dinitrotoluenes can be recovered in excellent yield.
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Inventors:
Rosenblatt, David H. (Baltimore, MD, US) Dennis, Jr., William H. (Braddock Heights, MD, US)
Application Number:
529873
Filing Date: 1974-12-05 Publication_date: 1976-01-06 Assignee:
The United States of America as represented by the Secretary of the Army (Washington, DC)
Primary Class(es):
568/934
Other Classes:
US Patent Ref:
Other Refs:
Primary Examiner:
Sebastian, Leland A.
Assistant Examiner:
Attorney:
Edelberg; Nathan, Gibson; Robert P., Erkkila; A. Victor
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